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By John B. Wachtman

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Figure 2 shows that there is only a gradual pH change until all of the ferric iron is precipitated. The volume of titrant consumed to reach the end point includes the sum of the free acid contribution and the ferric iron contribution. There is no usable break to separate the free acid end point from the ferric iron. Figure 3 illustrates the benefit derived from the reduction of the ferric iron. A sharp break is evident from pH 3 to pH 6 . This break represents the equivalencepoint of the free acid titration.

S. in chemistry and an MBA degree from Cleveland State University. He first joined Ferro as a lab technician then served four years as supervisor of sheet steel development before assuming his present duties in 1985. 367 The actual enamel system was then developed with the cooperation of the water heater manufacturer and frit powder suppliers so that the coating passes the necessary durability requirements. The Enamel System The enamel system developed for electrostatic application has water resistance comparable to conventional wet process enamels.

Bayer AG and Bosch-Siemens have defined specific test methods and tolerances. The laboratory methods for quality control at Bayer and for incoming material control at Bosch-Siemens have been correlated so that the results from both are directly comparable. In addition to the enamel powder properties, the physical properties of the fired enamel (AR, color, surface quality, and bond) are defined in the specifications and are continuously controlled. Energy Utilization The development and use of fiber-lined furnaces with a limited amount of air motion or draft has reduced energy consumption.

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49th Porcelain Enamel Institute Technical Forum by John B. Wachtman


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